000			01933cam a2200313 i 4500
003			EG-ScBUE
005			20260105101311.0
008			160917t2017 enka f b 001 0 eng d
020			_a9780128095812
040			_aIDEBK _beng _erda _cIDEBK _dOCLCO _dUk _dEG-ScBUE
082	0	4	_a547 _bPIR _222
100	1		_aPirrung, Michael, _eauthor.
245	1	0	_aHandbook of synthetic organic chemistry / _cMichael C. Pirrung.
246	3	0	_aSynthetic organic chemistry
250			_aSecond edition.
264		1	_aLondon : _bAcademic Press, / Elsevier, _c[2017]
264		4	_cc2017
300			_axii, 272 pages : _billustrations (some color) ; _c24 cm
336			_2rdacontent _atext _btxt
337			_aunmediated _2rdamedia _bn
338			_avolume _bnc _2rdacarrier
504			_aIncludes bibliographical references and index.
505	0		_a1. Safety<br>2. Searching the literature<br>3. Reagents<br>4. Gases<br>5. Reactions on a small scale -- 1-25 mmol<br>6. Temperature control<br>7. Solvents<br>8. The research notebook<br>9. Conducting the reaction itself<br>10. Following the reaction<br>11. Working up reactions<br>12. Evaporation<br>13. Vacuum systems<br>14. Purification of products<br>15. Methods for structure elucidation<br>16. Cleaning up after the reaction<br>17. Specific examples<br>18. Strategies for reaction optimization<br>Appendices<br>1. Safety protocols<br>2. Synthetic solvent selection chart<br>3. Solvent miscibility<br>4. Freezing points of common organic solvents<br>5. Toxicities of common organic solvents<br>6. Recipes for TLC stains<br>7. NMR spectral data of common contaminants of organic and organometallic reaction products<br>8. Acidities of organic functional groups<br>9. Acidities of organic functional groups in DMSO<br>10. Stuck joints
650		7	_aOrganic compounds _xSynthesis. _2BUEsh _941977
651			_2BUEsh
653			_bENGCHE _cMarch2019
655			_vReading book
942			_2ddc _cBB
999			_c27250 _d27221